Journal of Lanzhou University of Technology ›› 2026, Vol. 52 ›› Issue (2): 8-15.

• Materials Science and Engineering • Previous Articles     Next Articles

Effect of solution treatment and aging on the tribological properties of K444 alloy in a wide temperature range

XIAO Rong-zhen1, CHEN Yang-yang1, CHEN Han-feng2, WANG Jiang2, LIU Jun-zhao1   

  1. 1. State Key Laboratory of Advanced Processing and Recycling of Non-ferrous Metals, Lanzhou University of Technology, Lanzhou 730050, China;
    2. National Key Laboratory of Ni&Co Associated Minerals Resources Development and Comprehensive Vtilization,Jinchuan Group Co., Ltd., Jinchang 737100, China
  • Received:2025-04-20 Online:2026-04-28 Published:2026-04-28

Abstract: The tribological properties and wear mechanisms of K444 alloy after heat treatment were investigated using Si3N4 balls as the counterface material over a wide temperature range (RT-800 ℃). The research results showed that the heat treatment process induces the dissolution of the γ′-strengthening phase and the precipitation of the η phase, increasing the hardness of the material from 41.8 HRC in the as-cast state to 45.4 HRC in the aged state. From room temperature to 600 ℃, the wear rate of K444 alloy remains at a low level, on the order of 10-6 mm3·m-1 ·N-1 . After solution aging treatment, the wear rate of the alloy is significantly reduced, which is attributed to the re-solution of the γ' strengthening phase and the precipitation of fine and uniform η phase during cooling, significantly improving the wear resistance of the alloy. Microscopic characterization confirms that the in-situ formed dense Cr2O3 oxide film during friction is the core mechanism for improving wear resistance. When the temperature rises to 800 ℃, the tribological properties of K444 alloy deteriorate significantly, and thewear rates of both the as-cast and heat-treated alloys increase to the order of 10-5 mm3·m-1·N-1, with the oxidation wear mechanism becoming dominant due to the failure of the dynamic balance of the oxide layer.

Key words: solution treatment, aging treatment, friction and wear, wide temperature range, K444

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